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1 H NMR Titrations of SNAC with 50 mM CTAB Samples were prepared by creating a stock solution of SNAC (36 mg, 120 mmol) and its conjugate acid (8.4 mg, 30 mM) in MeOH (2.0 mL), and a solution of CTAB (91 mg, 250 mmol) and sodium trimethylsilylpropanesulfonate (DSS) (2.2 mg, 10 mmol) in D 2 O (5.0 mL)
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